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The calcination temperature exerted a large effect on the morphology of sintered LATP pellets, even though the sintering temperature was same for all the samples. Formation of voids was observed in the precursor powders calcined at 500, 600, 700, and 900C, while no void was formed in the powder calcined at 800C. The precursor powders calcined at low temperatures
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26.02.2014This preparation method is calcination-free, and the resulting MnCo2O4 microspheres were surprisingly assembled by nanoparticles and nanosheets. Two kinds of MnCo2O4 crystal nucleus with different exposed facet of (1̅10) and (11̅2̅) could be responsible for the formation of particle-assembled and sheet-assembled microspheres, respectively. Profiting
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30.03.2015Calcination temperature obviously affects the light absorption characteristics of NSC-TiO 2-x samples, as shown in Fig. 9. As can be seen from Fig. 9, an obviously red shift was observed for all NSC-TiO 2-x samples, and its visible absorption intensity decreased with the increase of calcination temperature, which can be explained by the
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01.03.2019Ranging from 4000 to 400 cm −1, the FT-IR spectra of the as-synthesized catalyst and its calcined counterparts were recorded (Fig. 2A). The peak at 3489 cm −1 is attributed to the stretching mode of the bonded and structurally intercalated water molecules and their bending vibrations were observed at 1660 and 1622 cm −1.The peaks at 3145 and 3048 cm −1 were
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